Two-dimensional TOCSY spectrum of dogfish a-crystallin. A
: The NH to α, β and γ 1
H proton region of the TOCSY spectrum of dogfish α-crystallin at 25 °C. The assignments are indicated for the αB subunit.
: Deviation from random coil chemical shifts [26
] for the α-CH 1
H resonances of the COOH-terminal extension of dogfish α-crystallin.